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Central and State Pollution Control Board recruitment Environmental Monitoring & Instrumental Analysis: practice questions

Central and State Pollution Control Board recruitment (Scientist, Environmental Engineer, AEE) · India · Central Pollution Control Board and State Pollution Control Boards / state PSCs

Original practice questions written to the published syllabus · not past papers
7worked here, free
23written to this exam in this subject
9syllabus units

What this subject covers

How environmental samples are taken and analysed and how good the numbers are: sampling plans, gravimetric and volumetric methods, spectroscopy, chromatography, quality assurance and monitoring networks.

In the exams: UGC NET Environmental Sciences Unit 2; ICAR AIEEA-PG Physical Science Unit II (instrumental analysis); ICAR AICE Aquatic Environmental Management Unit 3

Where the 23 questions fall

How our questions for Central and State Pollution Control Board recruitment spread across the units of Environmental Monitoring & Instrumental Analysis. Difficulty: 6 easy, 15 medium, 2 hard.

Sampling and preservation of water, soil, air and biota5
Quality assurance, quality control and laboratory accreditation4
Monitoring objectives and network design3
Gravimetric and volumetric analysis3
Continuous and low-cost sensor monitoring3
Atomic absorption and ICP techniques2
UV-visible spectrophotometry and colorimetry1
Electrochemical methods and sensors1
Detection limits, accuracy, precision and calibration1

7 practice questions, worked

Choose an answer, then open the working. Each explanation says why the right answer is right and why the others are not.

1 · Monitoring objectives and network design · medium

What does the US EPA's data quality objectives process require before sampling begins?

  1. Buying the most sensitive instrument available
  2. Collecting as many samples as the budget allows
  3. Defining the decision and tolerable errors
  4. Choosing sites that are easiest to reach
Answer and working

C. Defining the decision and tolerable errors

DQOs derive sampling design from the decision and acceptable errors, not from convenience.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

2 · Sampling and preservation of water, soil, air and biota · easy

How should water samples for dissolved metal analysis usually be preserved?

  1. Treated with sulphuric acid and heated to 100 °C
  2. Frozen with sodium thiosulphate
  3. Left at room temperature in glass bottles
  4. Filtration and nitric acid to pH below 2
Answer and working

D. Filtration and nitric acid to pH below 2

Nitric acid keeps metals in solution and prevents adsorption; thiosulphate is for chlorinated microbiological samples.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

3 · Sampling and preservation of water, soil, air and biota · hard

What is isokinetic sampling in stack monitoring?

  1. Sampling at constant temperature to avoid condensation
  2. Sampling at the same time every day for comparability
  3. Sampling at the stack gas velocity
  4. Sampling with equal volumes from several stacks
Answer and working

C. Sampling at the stack gas velocity

Faster or slower sampling would under- or over-collect large particles because of their inertia.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

4 · UV-visible spectrophotometry and colorimetry · medium

Hexavalent chromium is commonly measured colorimetrically using

  1. Ammonium molybdate
  2. Nessler's reagent
  3. 1,5-diphenylcarbazide in acid
  4. Eriochrome Black T
Answer and working

C. 1,5-diphenylcarbazide in acid

Diphenylcarbazide forms a red-violet complex with Cr(VI) at about 540 nm.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

5 · Electrochemical methods and sensors · medium

Which electrode is a standard method for measuring fluoride in drinking water?

  1. Platinum ORP electrode
  2. Glass pH electrode
  3. Lanthanum fluoride ISE
  4. Clark oxygen electrode
Answer and working

C. Lanthanum fluoride ISE

The LaF3 crystal ISE responds to fluoride; TISAB fixes ionic strength and releases complexed fluoride.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

6 · Quality assurance, quality control and laboratory accreditation · easy

Which QC sample detects contamination introduced during field handling and transport?

  1. Calibration standard
  2. Field blank
  3. Certified reference material
  4. Matrix spike
Answer and working

B. Field blank

Field blanks are analyte-free water taken through field procedures; spikes test recovery; CRMs test accuracy.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

7 · Continuous and low-cost sensor monitoring · easy

Beta attenuation monitors are used to measure

  1. radon in homes
  2. particulate matter mass concentration
  3. noise levels
  4. dissolved oxygen
Answer and working

B. particulate matter mass concentration

BAMs measure the attenuation of beta radiation by particles collected on filter tape.

Further reading: See the manual sources: Standard Methods; Harris; Skoog et al.; CPCB monitoring guidelines; ISO/IEC 17025

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Read the subject

Environmental Monitoring & Instrumental AnalysisThe full study manual, free Central and State Pollution Control Board recruitmentFormat, sections and how it has changed

More Central and State Pollution Control Board recruitment practice

Circular Economy & Bio-based ResourcesAir & Noise Pollution: Monitoring & Control

Environmental Monitoring & Instrumental Analysis for other exams

UGC NET · IndiaICAR AICE-JRF/SRF · IndiaCUET-PG · IndiaCUET-UG · India

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