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ICAR AICE-JRF/SRF Spices, Herbs, Essential Oils & Flavour Technology: practice questions

ICAR AICE-JRF/SRF (PhD) — Food Processing Technology, Food Safety & Quality, Processing and Food Engineering · India · ICAR through the National Testing Agency

Original practice questions written to the published syllabus · not past papers
10worked here, free
61written to this exam in this subject
11syllabus units

What this subject covers

Processing spices and herbs, extracting essential oils and oleoresins, and the technology of natural and synthetic flavours and food colours, including encapsulation and flavour stability.

In the exams: GATE XE-G Section 3 (spice; extraction of essential oils and oleoresins from spices); ICAR AIEEA-PG Code 18 Unit III (flavouring and pigment technology); ICAR AICE 35.a Unit 7

What ICAR AICE-JRF/SRF asks from it

ICAR AICE-JRF/SRF (PhD) — Food Processing Technology, Food Safety & Quality, Processing and Food Engineering

35.a Unit 7 covers plantation crops and spices processing. Expect deeper questions on extraction thermodynamics and selectivity, supercritical fluid processing, encapsulation and controlled release, reaction-flavour chemistry and its contaminants, authenticity testing, microbial decontamination options and mycotoxin control.

Where the 61 questions fall

How our questions for ICAR AICE-JRF/SRF spread across the units of Spices, Herbs, Essential Oils & Flavour Technology. Difficulty: 12 easy, 29 medium, 20 hard.

Natural, nature-identical and artificial flavours9
Natural colours and pigment technology9
Flavour encapsulation and delivery8
Process flavours and reaction flavours8
Medicinal and aromatic plants in foods8
Cryogenic grinding4
Oleoresins: solvent and supercritical CO2 extraction4
Major spices: composition and active principles3
Spice processing: cleaning, drying, grinding and sterilisation3
Essential oils: steam distillation and other extraction methods3
Quality standards and adulteration of spices2

10 practice questions, worked

Choose an answer, then open the working. Each explanation says why the right answer is right and why the others are not.

1 · Cryogenic grinding · medium

In a cryogenic grinding line, the screw conveyor before the mill in which liquid nitrogen is sprayed onto the spice is the

  1. Cyclone separator
  2. Classifier sieve
  3. Precooler
  4. Rotary airlock
Answer and working

C. Precooler

The precooler, usually an insulated screw conveyor with nitrogen spray, brings the spice to grinding temperature before the mill. The cyclone separates powder from gas, the sieve classifies the product, and an airlock meters material.

Further reading: Peter (ed.), Handbook of Herbs and Spices

2 · Essential oils: steam distillation and other extraction methods · hard

In steam distillation at atmospheric pressure, an oil component of molar mass 136 g/mol has a vapour pressure of 4.0 kPa and water 97.3 kPa at the boiling temperature. The mass of oil distilled per kg of water condensed is closest to

  1. 0.31 kg
  2. 0.041 kg
  3. 0.0054 kg
  4. 7.6 kg
Answer and working

A. 0.31 kg

m_oil/m_water = (P_oil × M_oil)/(P_water × M_water) = (4.0 × 136)/(97.3 × 18) = 544/1751 = 0.31 kg per kg water. 0.041 kg ignores the molar masses (4.0/97.3); 0.0054 kg inverts the molar mass ratio; 7.6 kg multiplies by 136/18 without the pressure ratio.

Further reading: Baser and Buchbauer (eds), Handbook of Essential Oils

3 · Essential oils: steam distillation and other extraction methods · hard

Folded (deterpenated) citrus oils are made because removing terpene hydrocarbons

  1. Removes the oxygenated compounds that carry the off-notes
  2. Raises the content of limonene in the oil
  3. Better stability and solubility
  4. Converts the oil into a water-insoluble resin
Answer and working

C. Better stability and solubility

Terpene hydrocarbons such as limonene contribute little odour, oxidise easily and dissolve poorly in water and dilute alcohol; removing them concentrates the oxygenated flavour compounds and improves stability and solubility. Folding lowers, not raises, limonene.

Further reading: Baser and Buchbauer (eds), Handbook of Essential Oils

4 · Oleoresins: solvent and supercritical CO2 extraction · medium

A spice gives 12% oleoresin. Taking yield as the only basis, 0.5 kg of this oleoresin carries the extractable flavour of about how much ground spice?

  1. 0.06 kg
  2. 6.0 kg
  3. 2.4 kg
  4. 4.2 kg
Answer and working

D. 4.2 kg

Spice = 0.5 ÷ 0.12 = 4.17 kg. 0.06 kg multiplies 0.5 by 0.12; 6.0 kg multiplies 0.5 by 12; 2.4 kg divides 12 by 5. In practice replacement ratios are confirmed by sensory and chemical comparison.

Further reading: Mukhopadhyay, Natural Extracts Using Supercritical Carbon Dioxide

5 · Natural, nature-identical and artificial flavours · easy

Retronasal aroma is perceived when

  1. Taste buds detect bitter compounds
  2. Pungent compounds stimulate pain receptors
  3. Volatiles reach the nose from the mouth
  4. The food is sniffed before eating
Answer and working

C. Volatiles reach the nose from the mouth

Retronasal olfaction occurs when volatiles released during chewing travel from the back of the mouth to the olfactory epithelium. Sniffing is orthonasal; taste buds and pain receptors give taste and chemesthesis.

Further reading: Reineccius, Flavor Chemistry and Technology

6 · Process flavours and reaction flavours · easy

Process (reaction) flavours are produced mainly by heating

  1. Reducing sugars with amino acids
  2. Fats with strong mineral acids
  3. Essential oils with ethanol
  4. Proteins with sodium chloride
Answer and working

A. Reducing sugars with amino acids

Heating reducing sugars with amino compounds drives the Maillard reaction that gives roasted, meaty and bready flavours. The other combinations do not describe process flavour manufacture.

Further reading: Reineccius, Flavor Chemistry and Technology

7 · Process flavours and reaction flavours · medium

A meaty reaction flavour is made by heating ribose with which amino acid?

  1. Cysteine
  2. Proline
  3. Leucine
  4. Glycine
Answer and working

A. Cysteine

Cysteine supplies sulphur that forms thiazoles, thiophenes and thiols with meaty character. Proline gives bready notes, leucine gives malty 3-methylbutanal, and glycine gives general roasted notes without meatiness.

Further reading: Reineccius, Flavor Chemistry and Technology

8 · Natural colours and pigment technology · medium

Curcumin used to colour a product turns red-brown when the product is

  1. Acidified
  2. Alkaline
  3. Frozen
  4. Salted
Answer and working

B. Alkaline

Curcumin is yellow in acid and neutral conditions and red-brown in alkaline conditions. Freezing and salting do not change its colour in this way.

Further reading: Delgado-Vargas and Paredes-López, Natural Colorants

9 · Medicinal and aromatic plants in foods · easy

Menthol is obtained mainly from

  1. Cymbopogon flexuosus
  2. Mentha arvensis
  3. Ocimum tenuiflorum
  4. Withania somnifera
Answer and working

B. Mentha arvensis

Japanese or corn mint, Mentha arvensis, is the main source of natural menthol. Cymbopogon species are lemongrass (citral), Ocimum tenuiflorum is tulsi, and Withania somnifera is ashwagandha.

Further reading: Peter (ed.), Handbook of Herbs and Spices

10 · Quality standards and adulteration of spices · medium

A 1 g sample of ground pepper contains 50 mg of piperine. Its piperine content is

  1. 5.0%
  2. 0.5%
  3. 50%
  4. 2.0%
Answer and working

A. 5.0%

50 mg ÷ 1000 mg × 100 = 5.0%. 0.5% misplaces the decimal; 50% treats mg as per cent; 2.0% inverts and scales wrongly.

Further reading: FSSAI, DART: Detect Adulteration with Rapid Test

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Read the subject

Spices, Herbs, Essential Oils & Flavour TechnologyThe full study manual, free ICAR AICE-JRF/SRFFormat, sections and how it has changed

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