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ICAR AICE-JRF/SRF Statistics, Experimental Design & Chemometrics for Food Science: practice questions

ICAR AICE-JRF/SRF (PhD) — Food Processing Technology, Food Safety & Quality, Processing and Food Engineering · India · ICAR through the National Testing Agency

Original practice questions written to the published syllabus · not past papers
10worked here, free
93written to this exam in this subject
9syllabus units

What this subject covers

Probability, inference and the designs used in food research and quality work: factorial and response-surface designs for formulation and process optimisation, mixture designs, the statistics of sensory panels, and multivariate methods (PCA, PLS) used with spectra and chromatograms. Goes further than the general statistics subjects in Agricultural Engineering (probability-statistics-data) and Agribusiness (business-statistics) by focusing on food formulation, sensory and analytical data.

In the exams: Applied throughout ICAR AICE-JRF/SRF research units and every PG thesis; probability and statistics also appear in GATE XE-A

Where the 93 questions fall

How our questions for ICAR AICE-JRF/SRF spread across the units of Statistics, Experimental Design & Chemometrics for Food Science. Difficulty: 27 easy, 44 medium, 22 hard.

Factorial and fractional factorial designs11
Response surface methodology: central composite and Box-Behnken designs11
Multivariate methods: principal component analysis, cluster analysis and partial least squares11
Analysis of variance: one-way, two-way and multiple comparisons10
Completely randomised, randomised block and Latin square designs10
Mixture designs for formulation10
Non-parametric tests used with sensory data10
Calibration, limit of detection and measurement uncertainty basics10
Statistical software and reproducible data analysis10

10 practice questions, worked

Choose an answer, then open the working. Each explanation says why the right answer is right and why the others are not.

1 · Analysis of variance: one-way, two-way and multiple comparisons · easy

Which is an assumption of the standard ANOVA F test?

  1. Equal treatment means in the population
  2. Correlated errors within each group
  3. Equal variances among the treatment groups
  4. Exactly normal raw data before any fitting
Answer and working

C. Equal variances among the treatment groups

ANOVA assumes independent errors, approximately normal residuals and equal variances. Equal means is the null hypothesis being tested, not an assumption; correlated errors violate independence; normality refers to residuals, approximately.

Further reading: Montgomery, Design and Analysis of Experiments; Gomez and Gomez, Statistical Procedures for Agricultural Research

2 · Completely randomised, randomised block and Latin square designs · medium

An assessor can taste only three of seven samples in a session without fatigue. Which design family handles this?

  1. Randomised complete block design
  2. Completely randomised design
  3. Full 2^7 factorial design
  4. Balanced incomplete block design
Answer and working

D. Balanced incomplete block design

When a block (session) cannot hold all treatments, incomplete block designs allocate subsets so that every pair appears together equally often. A complete block would need all seven samples per session.

Further reading: Gomez and Gomez, Statistical Procedures for Agricultural Research; Montgomery, Design and Analysis of Experiments

3 · Response surface methodology: central composite and Box-Behnken designs · medium

How many runs has a central composite design for three factors with six centre points?

  1. 20
  2. 14
  3. 26
  4. 15
Answer and working

A. 20

CCD = 2^k + 2k + centre = 8 + 6 + 6 = 20. 14 omits the centre points; 26 uses 3^k minus one; 15 is the usual Box-Behnken size for three factors.

Further reading: Myers, Montgomery and Anderson-Cook, Response Surface Methodology

4 · Response surface methodology: central composite and Box-Behnken designs · hard

In response surface analysis, what does the lack-of-fit test compare?

  1. The R² of the model against the adjusted R² of a model with fewer terms in it
  2. The predicted optimum against the verification run made at the optimum settings
  3. The variance of the factorial points against the variance of the axial points
  4. Residual error not explained by the model against pure error from replicated runs
Answer and working

D. Residual error not explained by the model against pure error from replicated runs

Lack of fit splits residual error into pure error (from replicated centre points) and lack-of-fit error. A significant lack of fit means the model form is inadequate. R² comparisons and verification runs are separate checks.

Further reading: Myers, Montgomery and Anderson-Cook, Response Surface Methodology

5 · Mixture designs for formulation · medium

Why does a Scheffé mixture model have no intercept term?

  1. The proportions sum to one, so an intercept is redundant with the linear terms
  2. Because mixtures always give a zero response when all components are present
  3. Because the intercept is replaced by the pure-error term from the centroid run
  4. Because an intercept would make the model rotatable, which mixtures must avoid
Answer and working

A. The proportions sum to one, so an intercept is redundant with the linear terms

With Σxi = 1, a constant b0 can be absorbed into the linear terms (b0 = b0Σxi), so it cannot be estimated separately. The other reasons are false.

Further reading: Cornell, Experiments with Mixtures

6 · Mixture designs for formulation · easy

For a four-component mixture, what shape is the experimental region when every component may range from 0 to 1?

  1. A triangle
  2. A cube
  3. A square
  4. A tetrahedron
Answer and working

D. A tetrahedron

The simplex for q components has q − 1 dimensions: a triangle for three components and a tetrahedron for four. A cube is the region of three independent factors.

Further reading: Cornell, Experiments with Mixtures

7 · Non-parametric tests used with sensory data · easy

Liking scores for one product come from two separate consumer groups that are not normally distributed. Which test compares the groups?

  1. Wilcoxon signed-rank test
  2. Friedman test
  3. McNemar test
  4. Mann-Whitney U test
Answer and working

D. Mann-Whitney U test

Two independent groups with non-normal data call for the Mann-Whitney U (Wilcoxon rank-sum) test. The signed-rank and McNemar tests are for paired data; Friedman for three or more related samples.

Further reading: Næs, Brockhoff and Tomic, Statistics for Sensory and Consumer Science

8 · Non-parametric tests used with sensory data · medium

Which statistic measures agreement among several assessors' rankings of the same products?

  1. Pearson's correlation between the first two assessors only
  2. The coefficient of variation of each assessor's ranks
  3. Kendall's coefficient of concordance, W, across all assessors
  4. The chi-square goodness-of-fit statistic of the rank totals
Answer and working

C. Kendall's coefficient of concordance, W, across all assessors

Kendall's W ranges from 0 (no agreement) to 1 (complete agreement) among all assessors and is used to check panel consistency.

Further reading: Næs, Brockhoff and Tomic, Statistics for Sensory and Consumer Science

9 · Non-parametric tests used with sensory data · hard

Ten assessors rank three products; rank sums are 15, 20 and 25. Using the Friedman statistic 12/[bt(t + 1)] ΣR² − 3b(t + 1), and a critical chi-square of 5.99 (2 df, α = 0.05), what is the result?

  1. 5.0; significant
  2. 5.0; not significant
  3. 125.0; significant
  4. 2.5; not significant
Answer and working

B. 5.0; not significant

12/(10 × 3 × 4) = 0.1; ΣR² = 225 + 400 + 625 = 1,250; 0.1 × 1,250 = 125; minus 3 × 10 × 4 = 120 gives 5.0, below 5.99, so not significant. 125.0 forgets to subtract 120; 2.5 halves the statistic.

Further reading: Næs, Brockhoff and Tomic, Statistics for Sensory and Consumer Science

10 · Statistical software and reproducible data analysis · easy

What is the purpose of version control for analysis scripts?

  1. To compress data files so they occupy less storage on the server
  2. To speed up statistical calculations on large data sets
  3. To record every change, so earlier versions are recoverable
  4. To translate scripts between programming languages automatically
Answer and working

C. To record every change, so earlier versions are recoverable

Version control tracks the history of scripts, who changed what and when, and allows any earlier state to be restored.

Further reading: Montgomery, Design and Analysis of Experiments; Næs, Brockhoff and Tomic, Statistics for Sensory and Consumer Science

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Statistics, Experimental Design & Chemometrics for Food ScienceThe full study manual, free ICAR AICE-JRF/SRFFormat, sections and how it has changed

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