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ICAR AICE-JRF/SRF Food Quality Assurance, Statistical Process Control & Laboratory Accreditation: practice questions

ICAR AICE-JRF/SRF (PhD) — Food Processing Technology, Food Safety & Quality, Processing and Food Engineering · India · ICAR through the National Testing Agency

Original practice questions written to the published syllabus · not past papers
10worked here, free
80written to this exam in this subject
14syllabus units

What this subject covers

Controlling quality in the plant and in the laboratory: quality systems and TQM, control charts and process capability, acceptance sampling and two- and three-class sampling plans, laboratory quality management and ISO/IEC 17025 accreditation, method validation and proficiency testing.

In the exams: ICAR AICE 35.a Unit 4 (quality systems, control charts, acceptance sampling) and 35.b Units 1 and 3 (ISO 17025, NABL accreditation, 2- and 3-class sampling plans); food analyst examinations

Where the 80 questions fall

How our questions for ICAR AICE-JRF/SRF spread across the units of Food Quality Assurance, Statistical Process Control & Laboratory Accreditation. Difficulty: 18 easy, 48 medium, 14 hard.

Statistical process control: control charts for variables and attributes9
Acceptance sampling and operating characteristic curves9
Two- and three-class microbiological sampling plans9
ISO 9001 quality management system8
Process capability indices8
Concepts of quality and quality systems7
Total quality management tools6
Laboratory quality management and ISO/IEC 170255
Method validation: accuracy, precision, LOD, LOQ and recovery4
Measurement uncertainty4
Laboratory accreditation bodies and their role4
Proficiency testing and reference materials3
Raw-material, in-process and finished-product quality control2
Non-destructive quality evaluation and online inspection2

10 practice questions, worked

Choose an answer, then open the working. Each explanation says why the right answer is right and why the others are not.

1 · ISO 9001 quality management system · medium

In ISO 9001:2015, what replaced the separate requirement for preventive action?

  1. Risk-based thinking
  2. Annual third-party testing of finished products
  3. Statistical process control on all production lines
  4. A mandatory quality manual for every site
Answer and working

A. Risk-based thinking

The 2015 edition embeds risk-based thinking (clause 6.1, actions to address risks and opportunities) and removed the preventive-action clause. The quality manual became optional; testing and SPC are not mandated.

Further reading: Juran's Quality Handbook; ISO 9001:2015

2 · ISO 9001 quality management system · easy

Which is one of the seven quality management principles in ISO 9000:2015?

  1. Evidence-based decision making
  2. Centralised control by inspectors
  3. Lowest-price purchasing
  4. Mass inspection of all output
Answer and working

A. Evidence-based decision making

The principles are customer focus, leadership, engagement of people, process approach, improvement, evidence-based decision making and relationship management. Mass inspection and lowest-price purchasing are practices Deming warned against.

Further reading: Juran's Quality Handbook; ISO 9001:2015

3 · Statistical process control: control charts for variables and attributes · hard

A laboratory plots one fat result per day on an individuals chart: mean 4.0%, mean moving range 0.15%. What are the control limits? (E₂ = 2.66)

  1. 3.55% to 4.45%
  2. 3.60% to 4.40%
  3. 3.70% to 4.30%
  4. 3.85% to 4.15%
Answer and working

B. 3.60% to 4.40%

Limits = X̄ ± 2.66 MR̄ = 4.0 ± 2.66 × 0.15 = 4.0 ± 0.40, i.e. 3.60% to 4.40%. 3.55 to 4.45 uses 3 × MR̄; 3.85 to 4.15 uses ±MR̄; 3.70 to 4.30 uses ±2MR̄.

Further reading: Montgomery, Introduction to Statistical Quality Control; ISO 2859-1

4 · Process capability indices · hard

A filler must keep the mean at least 3σ above a 500 g minimum. If σ falls from 2.0 g to 1.0 g, by how much can the target be lowered?

  1. 6 g
  2. 3 g
  3. 1 g
  4. 2 g
Answer and working

B. 3 g

Target = 500 + 3σ: 506 g at σ = 2.0, 503 g at σ = 1.0, a saving of 3 g per pack. 1 g is the change in σ; 6 g is the old safety margin; 2 g is the old σ.

Further reading: Montgomery, Introduction to Statistical Quality Control; ISO 2859-1

5 · Two- and three-class microbiological sampling plans · medium

For the same plan (n = 5, c = 2, m = 10², M = 10³ cfu/g), one unit gives 2000 cfu/g and the others are below 100. What is the decision?

  1. Accept: the average is below M
  2. Reject: one unit exceeds M
  3. Retest the high unit and use the lower value
  4. Accept: only one unit exceeds m
Answer and working

B. Reject: one unit exceeds M

Any unit above M makes the lot unacceptable regardless of c. Averaging or retesting to replace a result is not permitted by the plan.

Further reading: ICMSF, Microorganisms in Foods 7; Codex CXG 21-1997

6 · Non-destructive quality evaluation and online inspection · hard

Why do wet, salty products reduce the sensitivity of a metal detector?

  1. They make stainless steel pieces magnetic and harder to see
  2. They raise the conveyor belt speed automatically
  3. They absorb X-rays more strongly than dry products
  4. Their conductivity masks small metal
Answer and working

D. Their conductivity masks small metal

Conductive products give a signal of their own (product effect); the detector is adjusted to ignore it, which also reduces sensitivity to small metal, especially stainless steel. X-ray absorption is irrelevant to metal detection.

Further reading: Juran's Quality Handbook; ISO 9001:2015

7 · Laboratory quality management and ISO/IEC 17025 · medium

What new requirement did ISO/IEC 17025:2017 add for statements of conformity?

  1. That every result be tested in duplicate by two labs
  2. A documented decision rule that accounts for uncertainty
  3. That all results be reported without uncertainty
  4. That conformity statements be made only by regulators
Answer and working

B. A documented decision rule that accounts for uncertainty

When reporting conformity with a specification, the laboratory must define and agree the decision rule, including how measurement uncertainty is taken into account. The other options are not requirements.

Further reading: ISO/IEC 17025:2017; Eurachem guides; ISO 13528

8 · Proficiency testing and reference materials · hard

A laboratory reports 10.8 ± 0.6 (U, k = 2) against a reference value of 10.0 ± 0.3 (U). What is the En number, and is it satisfactory?

  1. 0.80; satisfactory
  2. 0.89; satisfactory
  3. 1.33; satisfactory
  4. 1.19; not satisfactory, since |En| > 1
Answer and working

D. 1.19; not satisfactory, since |En| > 1

En = (10.8 − 10.0)/√(0.6² + 0.3²) = 0.8/0.671 = 1.19, which exceeds 1. 0.89 adds the U values linearly; 1.33 divides by 0.6 alone and misjudges the rating; 0.80 omits the denominator.

Further reading: ISO/IEC 17025:2017; Eurachem guides; ISO 13528

9 · Proficiency testing and reference materials · medium

What distinguishes a certified reference material from an ordinary reference material?

  1. A higher price than in-house controls
  2. Production by the laboratory itself
  3. A matrix identical to every food tested
  4. A certificate with value, uncertainty and traceability
Answer and working

D. A certificate with value, uncertainty and traceability

A CRM is characterised by a metrologically valid procedure and carries a certificate stating the property value, its uncertainty and traceability. Price and matrix are not defining, and in-house materials are not certified.

Further reading: ISO/IEC 17025:2017; Eurachem guides; ISO 13528

10 · Laboratory accreditation bodies and their role · hard

Which Codex guideline recommends accreditation, proficiency testing, validated methods and internal QC for laboratories involved in import and export control of foods?

  1. CXG 27-1997
  2. CXC 1-1969
  3. CXG 50-2004
  4. CXG 21-1997
Answer and working

A. CXG 27-1997

CXG 27-1997 covers assessment of the competence of testing laboratories involved in import and export control. CXG 50-2004 is on sampling, CXG 21-1997 on microbiological criteria and CXC 1-1969 on food hygiene.

Further reading: ISO/IEC 17025:2017; Eurachem guides; ISO 13528

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Read the subject

Food Quality Assurance, Statistical Process Control & Laboratory AccreditationThe full study manual, free ICAR AICE-JRF/SRFFormat, sections and how it has changed

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